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Raman spectroscopy undoubtedly emerged as a relevant tool for probing and characterization of nanomaterials like nanosensor, nanotube and nanowire, as these are intensively studied in various areas of science due to their unique mechanical, electrical and chemical properties. For better understanding of nanomaterials like nanoceramic, nanocomposite, glassy material and semiconductor, techniques like micro Raman spectroscopy have been successfully applied for their better characterization.