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Capillary electrokinetic separation methods have been used in several formats (i.e. capillary zone electrophoresis (CZE), capillary isoelectric focusing (CIEF), capillary isotachophoresis (CI), and capillary gel electrophoresis (CGE)) to analyze and characterize a wide variety of analytes from simple inorganic ions, small organic molecules, peptides, to proteins, DNA and RNA. Capillary electrophoresis is becoming a valuable tool for the analysis of colloidal/nano particles because of its speed, simplicity, and separating capabilities.