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Reversible bond cleavage triggered by laser flash impulse is a typical pattern of the reaction of coordination compounds studied with LFP technique. Pulsed laser techniques are mainly well-suited for the investigation of the kinetics of ligand binding in respect of both energy required to vacate the coordination site on central ion as well as the time-resolution of the detection system, correlated with the flash-length.<br />Unsaturated transition metal complexes make a group of particular interest as they exemplify intermediates in a variety of chemical reactions. Application of LFP enables the formation of such compounds and determination of their binding abilities.