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As one of the main products of coal-to-ammonia enterprises, industrial ammonia water mainly comes from the recovery of ammonia-containing gas in the process of synthetic ammonia production and the deammonia-removing equipment of industrial wastewater. The impurities in the recovered ammonia water are high, and the content of total organic carbon, COD, volatile phenol and sulfide in the ammonia water seriously affects the quality of the industrial ammonia water, and increases the difficulty of the subsequent ammonia water quality improvement process. Therefore, the determination of total organic carbon content in industrial ammonia water is an important parameter in the production process of ammonia water upgrading.