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Nanoparticles continue to attract widespread attention in many scientific fields. The sizes and shapes of nanoparticles are important factors that determine their physical and chemical properties. It is well known that silver nanoparticles have superior properties relative to other nanostructured metal particles, such as their electrical conductivities, antimicrobial effects, optical properties, and applications in oxidative catalysis. This service provides a capillary electrophoresis (CE) method to separate silver particles in nanometer regimes. The combination of CE and DAD is a powerful one for the separation and characterization of various silver nanoparticles.