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The polymers of carbohydrates are disaccharides and polysaccharides that consist of two or more monomers respectively. Examples of monosaccharide are: glucose, fructose and galactose. Examples of disaccharides are: sucrose, lactose and maltose. Carbohydrates have become increasingly important commercially not only as food or structural building blocks, but also as natural health products. It is essential to have proper QC of carbohydrate-based therapeutics to ensure their efficacy and safety.