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Study of Characterization of Thin Metallic Films by Brillouin Scattering (CAT#: STEM-ST-0094-YJL)

Introduction

In the case of metallic films, often poor knowledge of the precise (within, let us say, 5 nm) thickness of the film has made the estimate of elastic constants, based on SBS exclusively, unsatisfactory. This imprecision has sometimes been due to unavoidable surface undulations (inhomogeneous thickness) connected with the deposition technique, and the presence of strong surface and interface roughness. Great improvements in the speed of the measurements in the presence of low SBS ripple cross sections, typical of metals, obtained by means of a new experimental apparatus, will be reported elsewhere. In recent years, grazing angle x-ray diffraction and x-ray reflectivity have been extensively used to study the structural properties of thin films and multilayers and the topography and morphology of their surfaces and interfaces.




Principle

From a quantum point of view, Brillouin scattering is an interaction of light photons with acoustic or vibrational quanta (phonons), with magnetic spin waves (magnons), or with other low frequency quasiparticles interacting with light. The interaction consists of an inelastic scattering process in which a phonon or magnon is either created (Stokes process) or annihilated (anti-Stokes process). The energy of the scattered light is slightly changed, that is decreased for a Stokes process and increased for an anti-Stokes process. This shift, known as the Brillouin shift, is equal to the energy of the interacting phonon and magnon and thus Brillouin scattering can be used to measure phonon and magnon energies.

Applications

Brillouin scattering is used to determine acoustic velocities and elastic properties of a number of crystalline solids, glasses, and liquids.

Procedure

1. Sample preparation
2. Measurement by scattering detection instrument
3. Data analysis

Materials

Brillouin scattering measurement system (Brillouin spectrometer)
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