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Thermal Conductivity Measurements of Carbon-Nanotube Suspensions by 3ω-method (CAT#: STEM-PPA-0044-WXH)

Introduction

A carbon nanotube (CNT) is a tube made of carbon with a diameter in the nanometer range (nanoscale). They are one of the allotropes of carbon.
CNTs are not easily suspended in polar solvents and are extremely hydrophobic materials, which has limited much of the solution processing to organic solvents, which also cannot afford high quality dispersions of CNTs. The current study has developed a variety of aqueous CNT solutions that employ surfactants, water-soluble polymers, or both to create suspensions of CNTs. These CNT 'ink' solutions were deposited with a variety of techniques that have afforded many interesting structures, both randomly oriented as well as highly ordered CNT architectures, and electroactive devices such as sensors were subsequently produced from these materials. The aqueous solutions developed contain some of the longest CNTs to be suspended in water, which have many benefits for electronic and mechanical properties of the resultant comp




Principle

The process involves a metal heater applied to the sample that is heated periodically. The temperature oscillations thus produced are then measured. The thermal conductivity and thermal diffusivity of the sample can be determined from their frequency dependence.

Applications

Determining the thermal conductivities of bulk material (i.e. solid or liquid) and thin layers

Procedure

1. Sample preparation and mounting
2. Experimental condition setting
3. Experiment start: Turn on the 3ω signal generator and lock-in amplifier, and control the temperature controller to make the sample temperature reach the set value. When the sample reaches a stable state, data acquisition and processing begin.
4. Data processing
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