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Measurement of Viscosity of Alkali Fluoride/Carbonate Eutectic Molten Salt by Rotating Viscometer Method (CAT#: STEM-PPA-0032-YJL)

Introduction

Molten salts have been regarded as one of the most promising media for concentrating solar power (CSP) system due to their excellent heat storage/transfer performances. Recently, heat storage/transfer media used at high temperature have been recommended for higher energy conversion efficiency. In pursuit of molten salt systems with high stability under high temperature, fluoride and carbonate molten salts are treated as the potential candidates for application.
Multicomponent fluoride molten salts generally melted above 400 °C and they remain thermal stable even though up to 1500 °C. It seems a good choice to use them at high temperature, but fluoride molten salts are so generally corrosive that the compatible materials is rarely available, moreover, they are expensive. On the contrary, molten carbonates are cheap and less corrosive, but their thermal stability range are so small (from 400 to 700 °C) that their application is limited. Therefore, researchers proposed to prepare the reciprocal molten salts of fluoride and carbonate which may have the advantages of the both molten salts. In fact, it is significant to obtain the accurate thermophysical parameters because they are necessary for the thermal hydraulic calculation and safety analysis of the CSP system, such as density, viscosity, and thermal conductivity.




Principle

The principle of the rotating viscometer method to measure the force acting on a rotor (torque) when it rotates at a constant angular velocity (rotational speed) in a liquid. Rotating viscometers are used for measuring the viscosity of Newtonian (shear-independent viscosity) or non-Newtonian liquids (shear dependent viscosity or apparent viscosity). Rotating viscometers can be divided in 2 groups, namely absolute and relative viscometers. In absolute viscometers the flow in the measuring geometry is well defined.
The measurements result in absolute viscosity values, which can be compared with any other absolute values. In relative viscometers the flow in the measuring geometry is not defined. The measurements result in relative viscosity values, which cannot be compared with absolute values or other relative values if not determined by the same relative viscometer method. Different measuring systems are available for given viscosity ranges as well as several rotational speeds.

Applications

Mineral oil industry; Food industry; Cosmetic/pharmaceutical industry; Petroleum industry; Chemical industry

Procedure

1. Pour the liquid into the measuring cup.
2. Insert the spindle into the liquid.
3. Rotate the spindle and measure the resistance.

Materials

• Sample Type: liquid, gel-like, or semi-solid everyday substances
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