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The service determined the 13 elements in human liver tissue by spark-source mass spectrometry. Spectral interferences are identified and calibration obtained by using carefully formulated synthetic standards. The relative standard deviation of this method is typically ± 9% for replicate analyses of a pooled liver ash obtained by oxygen plasma ashing, and ± 16% for replicate tissue samples taken through the whole analytical procedure. The accuracy of the method was checked by conducting complementary determinations by flame atomic absorption spectrometry.
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