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Thermal Conductivity Measurements of ytterbium doped CaF2 transparent ceramics by 3ω-method (CAT#: STEM-PPA-0048-WXH)

Introduction

Ytterbium-doped calcium fluoride transparent ceramics is considered as a promising laser gain medium.
Since the first YAG transparent ceramic for laser applications reported in 1995, which demonstrated the advantages of ceramics with respect to single crystals, rare earth-doped polycrystalline ceramics as solid-state laser host materials have been widely used and studied. Although Nd:YAG has become a leader material in the field of transparent ceramics and is nowadays industrially produced, a rare-earth-doped calcium fluoride matrix has been known as a host material for solid-state lasers since1964 and has experienced a renewed interest in the past decade, especially when doped with ytterbium cations, due to its excellent optical properties.




Principle

The process involves a metal heater applied to the sample that is heated periodically. The temperature oscillations thus produced are then measured. The thermal conductivity and thermal diffusivity of the sample can be determined from their frequency dependence.

Applications

Determining the thermal conductivities of bulk material (i.e. solid or liquid) and thin layers

Procedure

1. Sample preparation and mounting
2. Experimental condition setting
3. Experiment start: Turn on the 3ω signal generator and lock-in amplifier, and control the temperature controller to make the sample temperature reach the set value. When the sample reaches a stable state, data acquisition and processing begin.
4. Data processing
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