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Study on the Single-Crystal Elastic Properties of Zeolites by Brillouin Scattering (CAT#: STEM-ST-0118-YJL)

Introduction

Zeolites are both naturally occurring aluminosilicate minerals and important synthetic materials. They crystallize in a variety of low-density framework nanostructures built from corner-connected Al,SiO4 tetrahedra which define a narrow size distribution of pores and channels with molecular dimensions. These pores contain charge-balancing cations and molecular water. The increasing interest surrounding zeolite structures derives from their widespread industrial applications, such as pollution control, radioactive waste disposal, gas purification, and petroleum production. These applications make use of the unique physicochemical properties of zeolites, including selective ionic exchange, catalysis, and related molecular sieve properties.




Principle

From a quantum point of view, Brillouin scattering is an interaction of light photons with acoustic or vibrational quanta (phonons), with magnetic spin waves (magnons), or with other low frequency quasiparticles interacting with light. The interaction consists of an inelastic scattering process in which a phonon or magnon is either created (Stokes process) or annihilated (anti-Stokes process). The energy of the scattered light is slightly changed, that is decreased for a Stokes process and increased for an anti-Stokes process. This shift, known as the Brillouin shift, is equal to the energy of the interacting phonon and magnon and thus Brillouin scattering can be used to measure phonon and magnon energies.

Applications

Brillouin scattering is used to determine acoustic velocities and elastic properties of a number of crystalline solids, glasses, and liquids.

Procedure

1. Sample preparation
2. Measurement by scattering detection instrument
3. Data analysis

Materials

Brillouin scattering measurement system (Brillouin spectrometer)